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Synthesis of 4-(4,6-dimorpholino-1,3,5-triazin-2-yl) aniline
Author(s): 
Pages: 242-243
Year: Issue:  4
Journal: Qilu Pharmaceutical Affairs

Keyword:  三氯聚氰4-(46-二吗啉-135-三嗪-2-基)苯胺中间体合成;
Abstract: 目的 合成4-(4,6-二吗啉-1,3,5-三嗪-2-基)苯胺.方法 三氯聚氰与吗啉在冰浴条件下经取代反应制得4,4’-(6-氯-1,3,5-三嗪-2,4-二基)二吗啉,再与苯胺-4-硼酸频那醇酯经Suzuki反应制得4-(4,6-二吗啉-1,3,5-三嗪-2-基)苯胺.结果与结论 结构经核磁及质谱确证,总收率约61.7%.
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