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Determination of prim-O-glucasylcimifugin and 5-O-methylvisammioside in Fangfeng Tongsheng Pills by HPLC
Author(s): 
Pages: 525-526,545
Year: Issue:  9
Journal: QILU PHARMACEUTICAL AFFAIRS

Keyword:  防风通圣丸高效液相色谱法升麻素苷5-O-甲基维斯阿米醇苷;
Abstract: 目的 建立高效液相色谱法测定防风通圣丸中升麻素苷和5-O-甲基维斯阿米醇苷含量的方法.方法 色谱柱为Inertsil ODS-3(C18)(4.6 mm×250 mm,5 μm);流动相为甲醇-醋酸-水(35:4:61);检测波长为254 nm;流速为1.0 mL·min-1;柱温为室温.结果 升麻素苷进样量在0.147 2~0.736 0 μg之间,5-O-甲基维斯阿米醇苷进样量在0.134 ~0.670 μg之间与峰面积呈良好的线性关系(相关系数r分别为0.999 7、0.999 8);二者的平均回收率分别为99.78%和99.86%.结论 该方法 简便、准确,专属性好,可用于防风通圣丸的质量控制.
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